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Chemistry Education Lab Manuals

Determination of Lewis Acidity using 31P NMR:

Preparation and Characterisation of Metal Acetylacetonate Complexes

Synthesis of Aspirin

Aldol Condensation

Measuring Lipophilicity with NMR

Separation of Neutral, Acidic and Basic Compounds

Extraction of Essential Oils from Spices using Steam Distillation

Synthesis of p-Nitroaniline via a Multi-Step Sequence

Synthesis and Reactions of Ferrocene

Identification of an Alcohol using 13C NMR and DEPT

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Recent Posts

  • Phosphoramidite compound identification and impurity control by Benchtop NMR
  • Left with just a mg of your precious chemical? … still enough to verify your structure by NMR with a Spinsolve Carbon!
  • Lifting the curtain of undesired solvent signals – How solvent suppression and 13C decoupling remove the signals of regular protonated solvents from 1H NMR spectra to eliminate sample work-up before analysis.
  • Monitoring the oxidation of Phosphine ligands using 31P NMR
  • ACS Spring 2023 – March 26-30 – Indianapolis, IN & Hybrid

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