15. Differentiation of enantiomers by 2D NMR spectroscopy at 1T using residual dipolar couplings
Martin R. M. Koos, Ernesto Danieli, Federico Casanova, Bernhard Blümich, Burkhard Luy, Magnetic Resonance in Chemistry, (2016), 54 (6), 527-530, DOI: 10.1002/mrc.4222
Differentiating enantiomers using 2D bench-top NMR spectroscopy. Spectrometers working with permanent magnets at 1?T field strength allow the acquisition of 2D data sets. In conjunction with previously reported chiral alignment media, this setup allows the measurement of enantiomeric excess via residual dipolar couplings in stretched gelatine as a result of the reduced line width obtained by 2D J-resolved spectroscopy.