469. New Macrocyclic Bis-1,10-phenanthroline-2,9-dicarboxamides. Synthesis and Stereodynamics in Solution

Yu. A. Ustynyuk, V. S. Petrov, P. S. Lemport, V. A. Roznyatovsky, and V. G. Nenajdenko, Russian Journal of Organic Chemistry (2024), DOI: 10.1134/S1070428023100056

New macrocyclic 1,10-phenanthroline-2,9-dicarboxamide derivatives containing two phenanthroline cores were synthesized, and their structure was confirmed by NMR spectroscopy and other methods. The new macrocyclic phenanthrolines showed a complex stereodynamic behavior in solution, which was studied by ¹H NMR spectroscopy at different temperatures.